Methyl 2-amino-5-chlorobenzoate

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Methyl 2-amino-5-bromo­benzoate

In the title compound, C(8)H(8)BrNO(2), the dihedral angle between the aromatic ring and the methyl acetate side chain is 5.73 (12)°. The mol-ecular conformation is stabilized by an intra-molecular N-H⋯O hydrogen bond, generating an S(6) ring. In the crystal, mol-ecules are connected by N-H⋯O inter-actions, generating zigzag chains running along the b-axis direction.

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Methyl 2-amino-5-chloro­benzoate

The title compound, C(8)H(8)ClNO(2), is almost planar, with an r.m.s. deviation of 0.0410 Å from the plane through the non-hydrogen atoms. In the crystal structure, inter-molecular N-H⋯O hydrogen bonds link the mol-ecules into chains along the b axis. An intra-molecular N-H⋯O hydrogen bond results in the formation of a six-membered ring.

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Methyl 4-amino-2-chloro­pyrimidine-5-carboxyl­ate

In the title compound, C6H6ClN3O2, all non-H atoms are approximately coplanar [maximum deviation = 0.012 (4) Å]; an intra-molecular N-H⋯O hydrogen bond occurs between the amino group and the carbonyl group. In the crystal, mol-ecules are linked by N-H⋯N hydrogen bonds into supra-molecular chains propagated along [101].

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2-Amino-5-methyl-6-methyl­sulfanyl-4-phenyl­benzene-1,3-dicarbonitrile

The dihedral angle between the planes of the two aromatic rings of the title compound, C(16)H(13)N(3)S, is 56.7 (3)°. The crystal packing is stabilized by inter-molecular N-H⋯N hydrogen bonds, which link the mol-ecules into chains along [11[Formula: see text]].

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5 - Amino - 3 - methyl - 1 , 2 , 4 - thiadiazole

An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C-NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules.

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2010

ISSN: 1600-5368

DOI: 10.1107/s1600536810042510